目录 第1章 绪论1 Chapter 1 Introduction1 1.1 无机化学实验的目的1 1.1 Objectives of Inorganic Chemistry Experiment1 1.2 无机化学实验的学习方法2 1.2 Methods to Study Inorganic Chemistry Experiment4 1.3 学生实验守则6 1.3 Laboratory Rules for Students6 1.4 实验室安全守则8 1.4 Laboratory Safety Rules9 1.5 化学实验常用仪器介绍12 1.5 Frequently Used Laboratory Equipment16
第2章 基本操作训练20 Chapter 2 Basic Laboratory Techniques20 无机化学实验基本操作20 Basic Laboratory Techniques for Inorganic Chemistry Experiment20 2.1 常用玻璃仪器的洗涤和干燥20 2.1 Cleaning and Drying Glassware22 2.2 加热方法25 2.2 Heating28 2.3 容量仪器及其使用31 2.3 Volumetric Glassware34 2.4 化学试剂及其取用39 2.4 Transferring Chemical Reagents39 2.5 溶液的配制41 2.5 Preparing Solutions41 2.6 气体的发生、净化、干燥和收集42 2.6 Preparing, Purifying, Drying and Collecting Gases44 2.7 蒸发(浓缩)、结晶(重结晶)47 2.7 Evaporation (Concentration) and Crystallization (Recrystallization)47 2.8 结晶(沉淀)的分离和洗涤49 2.8 Separating a Liquid or Solution From a Solid52 2.9 试纸的使用56 2.9 Using Test Paper56 2.10 误差与数据处理58 2.10 Errors and Treatment of Data62 2.11 有效数字68 2.11 Significant Figures70 实验部分74 Experiments74 实验1 滴定操作练习74 Experiment 1 Titrimetric Analysis76 实验2 酸碱滴定79 Experiment 2 Acid-Base Titration80 实验3 EDTA标准溶液的配制与标定83 Experiment 3 Preparation and Standardization of an EDTA Solution84 实验4 水中钙、镁含量的测定(配位滴定法)86 Experiment 4 An Analysis of Concentrations of Calcium and Magnesium Ions in a Water Sample87
第3章 常数测定89 Chapter 3 Determination of the Constant89 实验5 化学反应速率和活化能89 Experiment 5 Determination of a Rate Law and Activation Energy92 实验6 弱酸电离常数测定(pH法)95 Experiment 6 Determination of Ionization Constant of Acetic Acid96 实验7 硫酸钡溶度积的测定(电导法)98 Experiment 7 Determination of the Solubility Product Constant of Barium Sulfate100 实验8 磺基水杨酸铁配合物的组成及稳定常数的测定104 Experiment 8 Determination of the Composition and the Stability Constant of an Iron(Ⅲ)-Sulfosalicylate Complex106 实验9 氧化还原反应110 Experiment 9 Oxidation-Reduction Reactions111
第4章 化合物的制备与提纯114 Chapter 4 Preparation and Purification of Compounds114 实验10 硫酸铜的提纯114 Experiment 10 Purification of Copper (Ⅱ) Sulfate116 实验11 氯化钠的提纯118 Experiment 11 Purification of Sodium Chloride119 实验12 氯化钾的提纯122 Experiment 12 Purification of Potassium Chloride123 实验13 硝酸钾的制备与提纯126 Experiment 13 Preparation and Purification of Potassium Nitrate127 实验14 明矾的制备130 Experiment 14 Synthesis of Potassium Alum131 实验15 莫尔盐(硫酸亚铁铵)的制备134 Experiment 15 Synthesis of Mohr’s Salt (Ammonium Ferrous Sulfate)135 实验16 草酸配合物的合成138 Experiment 16 Synthesis of Oxalate Complexes139 实验17 硫代硫酸钠的制备141 Experiment 17 Preparation of Sodium Thiosulfate143
第5章 元素及其化合物的性质145 Chapter 5 Properties of Elements and Compounds145 实验18 s区元素及其化合物145 Experiment 18 Elements in s-block and Their Compounds147 实验19 卤素及其化合物151 Experiment 19 Halogens and Their Compounds155 实验20 过氧化氢和硫的化合物159 Experiment 20 Hydrogen Peroxide and Compounds of Sulfur163 实验21 氮和磷167 Experiment 21 Nitrogen and Phosphorus171 实验22 ds区元素的化合物177 Experiment 22 Elements in ds-block and Their Compounds180 实验23 钛、钒、铬和锰的化合物184 Experiment 23 Compounds of Ti, V, Cr and Mn187 实验24 铁、钴、镍的化合物192 Experiment 24 Compounds of Fe, Co and Ni196 实验25 配合物202 Experiment 25 Coordination Compounds203
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