有机化学实验(双语版)(王红)9787122445513
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作者编者:王红//梁仁校//强根荣|责编:汪靓//宋林青
出版社化学工业
ISBN9787122445513
出版时间2024-03
装帧其他
开本其他
定价39.8元
货号31972861
上书时间2024-09-20
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目录
Chapter 1 Introduction of Experimental Organic Chemistry
1.1 The Role of Experimental Organic Chemistry
1.2 General Rules for the Organic Chemistry Experiments
1.3 Safety in the Organic Chemistry Laboratory
1.4 Pre-lab Reports.Notebooks and Lab Reports in the Laboratory
1.5 Common Laboratory Glassware and Equipment
1.6 The Literature of Organic Chemistry
1.7 Green Chemistry in the Organic Laboratory
Chapter 2 Basic Operations of Organic Chemistry Experiments
2.1 Heating and Cooling
2.2 Drying Organic Solutions and Solids
2.3 Filtration
2.4 Simple Distillation and Boiling Point
2.5 Fractional Distillation
2.6 Steam Distillation
2.7 Vacuum Distillation
2.8 Extraction and Washing
2.9 Recrystallization
2.10 Sublimation
2.11 Measurement of the Melting Point
2.12 Refluxing
2.13 Stirring Methods
2.14 Water-free and Air-free Operation
2.15 Chromatography Techniques
Chapter 3 Fundamental Experiments
3.1 Unsaturated Hydrocarbons
Exp.1 Preparation of Cyclohexene
Exp.2 Preparation of Phenylacetylene
3.2 Alkyl Halides
Exp.3 Preparation of 1-Bromobutane
Exp.4 Preparation of 2 Chloro 2 methylbutane
3.3 Alcohols，Phenols and Ethers
Exp.5 Preparation of 2-Methyl-2-butanol
Exp.6 Preparation of Triphenylmethanol
Exp.7 Preparation of Di n-butyl Ether
Exp.8 Preparation of Ethyl Phenyl Ether
Exp.9 Preparation of o-tert Butylhydroquinone
3.4 Aldehydes and Ketones
Exp.10 Preparation of Cyclohexanone
Exp.11 Preparation of Acetophenone
Exp.12 Preparation of Benzaldehyde
3.5 Carboxylic Acids
Exp.13 Preparation of Benzoic Acid
Exp.14 Preparation of Cinnamic Acid
Exp.15 Preparation of Hexane-1，6 dionic Acid
3.6 Carboxylic Acid Derivatives
Exp.16 Preparation of Ethyl Acetate
Exp.17 Preparation of nDibutyl Phthalate
3.7 Nitrogen-containing Compounds
Exp.18 Preparation of Acetanilide
Exp.19 Preparation of Methyl Orange
3.8 Heterocyclic Compounds
Exp.20 Preparation of 8-Hydroxyquinoline
Exp.21 Extraction and Separation of Caffeine from Tea Leaves
Chapter 4 Comprehensive Experiments
Exp.1 Preparation of Benzyl Alcohol and Benzoic Acid
Exp.2 Preparation of Benzil and Thin-layer Chromatography
Exp.3 Preparation of Acetylferrocene and Column Chromatography
Exp.4 Preparation of Ethyl Acetoacetate by the Claisen Condensation Reaction
Exp.5 Synthesis and Characterization of Aspirin
Exp.6 Multi-step Synthesis of Sulfanilamide
Exp.7 A Solvent Free Cannizzaro Reaction and Thin-layer Chromatography
Exp.8 Preparation of 4-Vinylbenzoic Acid by a Wittig Reaction
Exp.9 Preparation of Dimedone via the Robinson Annulation
Exp.10 Preparation of Cinnamic Acid by the Knoevenagel Condensation
Exp.11 Microwave assisted Preparation of Benzoic Acid and Ethyl Benzoate
Chapter 5 Experiments from Research and Literature
Exp.1 Synthesis of 3-Substituted Isoindolin-1-ones by Solvent-free Grinding Reaction
Exp.2 Electroorganic Synthesis of Nitriles
Exp.3 Ultrasonic Assisted Green Protocol for the Synthesis of N，N-bis Phenylsulfamide
Exp.4 Clean Synthesis in Water：Uncatalysed Preparation of Ylidenemalononitriles
Exp.5 Transition metal-catalyzed Convenient Synthesis of Internal Alkyne
Exp.6 N-Heterocyclic Carbene Catalyzed Intramolecular Benzoin Condensation to Access 9，10-Phenanthraquinone
Exp.7 Optical Resolution of （★）（S）-Methyl-（S）phenylsulfoximine with （+）-L-Camphorsulfonic Acid
Exp.8 Synthesis of Benzyl Acetate in Room Temperature lonic Liquids
Exp.9 Green Synthesis of 4-Bromoaniline
Exp.10 Pinacol Rearrangement and Photochemical Synthesis of Benzopinacol
Chapter 6 Study Guide of Some Typical Experiments
Exp.1 Preparation of Cyclohexene （Miniscale Reaction）
Exp.2 Preparation of.1
内容摘要
《有机化学实验（双语版）》全书共6章，分别为：有机化学实验的一般知识、有机化学实验的基本操作、有机化学基础性实验、有机化学综合性实验、研究性文献实验和典型实验的学习指导。本书在立足基本能力培养的同时，还补充完善了新型的有机合成技术和综合性实验内容，以实现知识、
能力的传承与创新协调发展。结合双语实验教学的特点和存在的问题，本书以英文为主，中文为辅，以期给读者提供一个相对完整的专业英语的学习环境，提升其专业英语的阅读、理解和书写能力。
本书可作为化学、化学工程与工艺、应用化学、能源化学工程、安全工程、材料科学与工程、生物制药、
环境科学等专业的双语教学配套实验教材，也可供留学生和相关专业人员参考。
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